Data quality metrics extracted from 4mi0.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 4MI0 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
CLSI BEAMLINE 08ID-1
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
CLSI
Beamline
_diffrn_source.pdbx_synchrotron_beamline
08ID-1
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2013-05-28
Detector
_diffrn_detector.type
RAYONIX MX300HE
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.28295
Software
Data collection
_software.classification
SBC-Collect
Data reduction
_software.classification
DENZO
Data scaling #1
_software.classification
SCALEPACK
Data scaling #2
_software.classification
HKL-3000
Model building
_software.classification
ARP/wARP (7.3.0)
Refinement #1
_software.classification
REFMAC (Garib N. Murshudov; garib@ysbl.york.ac.uk)
Refinement #2
_software.classification
BUSTER (2.10.0)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
45.010 57.796 74.542 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979041.28295 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 50.000 2.030
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.000 2.000
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.084 0.539
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 13445 635
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 19.40 1.80
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 98.0 94.1
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 4.6 4.2
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
4MI0
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2013-08-30
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
32.1 - 2.000 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1977 / 0.2387
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD