Data quality metrics extracted from 1lr0.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1LR0 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
ALS BEAMLINE 5.0.2
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
ALS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
5.0.2
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2001-04-30
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9791, 0.9611
Software
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
MLPHARE
Refinement
_software.classification
REFMAC (5.0)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 63 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
78.477 78.477 97.674 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979100.96110 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 19.840
High resolution limit [Å] 
_reflns.d_resolution_high
 1.914
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.083
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 13441
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 16.10
Completeness [%] 
_reflns.percent_possible_obs
 98.8
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1LR0
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2002-05-14
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
19.8 - 1.914 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1812 / 0.2228
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD