| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1994-09-15 |
Detector _diffrn_detector.type | RIGAKU RAXIS |
| Software | |
Data collection _software.classification | MSC (SOFTWARE) |
Data reduction _software.classification | MSC (SOFTWARE) |
Data scaling _software.classification | MSC |
Phasing _software.classification | SHELXL-93 |
Model building _software.classification | SHELXL-93 |
Refinement _software.classification | SHELXL-93 |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 31.97 65.08 27.25 94.57 111.56 82.98 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 20.000 |
High resolution limit [Å] _reflns.d_resolution_high | 1.100 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.095 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 36397 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 78.8 |
Multiplicity _reflns.pdbx_redundancy | 4.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1LKS |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-10-09 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 20.0 - 1.100 Å |