Data quality metrics extracted from 4lg0.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 4LG0 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
NSLS BEAMLINE X29A
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
NSLS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
X29A
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2012-06-12
Detector
_diffrn_detector.type
ADSC QUANTUM 315r
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.075,0.9793,0.979
Software
Data collection
_software.classification
ADSC (Quantum)
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
HKL-2000
Phasing
_software.classification
SHELXS
Refinement
_software.classification
REFMAC (5.8.0047)
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 2 2 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
68.658 114.944 136.325 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.075000.979300.97900 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 100.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.190
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.111
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 27722
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 24.10
Completeness [%] 
_reflns.percent_possible_obs
 99.5
Multiplicity 
_reflns.pdbx_redundancy
 12.0
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
4LG0
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2013-06-27
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
43.9 - 2.190 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1945 / 0.2430
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD