Data quality metrics extracted from 3lcu.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 3LCU at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
NSLS BEAMLINE X8C
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
NSLS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
X8C
Collection date
_diffrn_detector.pdbx_collection_date
2008-06-06
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9785, 0.9798, 0.9600
Software
Data reduction
_software.classification
DENZO (Zbyszek Otwinowski; hkl@hkl-xray.com)
Data scaling
_software.classification
SCALEPACK (Zbyszek Otwinowski; hkl@hkl-xray.com)
Refinement
_software.classification
CNS (Axel T. Brunger; axel.brunger@yale.edu)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 1 21 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
36.087 68.891 52.201 90.00 93.47 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
0.978500.979800.96000 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 50.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.100
  Rmerge -
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 28242
  <I/σ(I)> -
Completeness [%] 
_reflns.percent_possible_obs
 83.5
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
3LCU
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2010-01-11
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
50.0 - 2.100 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2046 / 0.2586
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD