Data quality metrics extracted from 1l8t.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1L8T at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
NSLS BEAMLINE X8C
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
NSLS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
X8C
Temperature [K]
_diffrn.ambient_temp
110
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2000-05-01
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.072
Software
Data reduction
_software.classification
DENZO
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
CNS
Refinement
_software.classification
CNS
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 43 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
46.629 46.629 301.289 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.541801.07200 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 40.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.400
Rmerge 
_reflns.pdbx_Rsym_value
 0.100
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 12532
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 8.00
Completeness [%] 
_reflns.percent_possible_obs
 88.4
Multiplicity 
_reflns.pdbx_redundancy
 7.3
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1L8T
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2002-03-21
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
40.0 - 2.400 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2340 / 0.2910
Structure solution method
_refine.pdbx_method_to_determine_struct
MOLECULAR REPLACEMENT
Starting model (for MR)
_refine.pdbx_starting_model
WARNING: no starting model (for MR) given