| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | ALS BEAMLINE 5.0.2 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | ALS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | 5.0.2 |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | PIXEL |
Collection date _diffrn_detector.pdbx_collection_date | 2018-06-19 |
Detector _diffrn_detector.type | DECTRIS PILATUS3 6M |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.97949 |
| Software | |
Data reduction _software.classification | XDS |
Data scaling _software.classification | Aimless |
Phasing _software.classification | CRANK2 |
Refinement _software.classification | PHENIX (dev_3936) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 31 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 126.364 126.364 104.334 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.97949 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 29.895 |
High resolution limit [Å] _reflns.d_resolution_high | 3.050 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.109 |
Rmeas _reflns.pdbx_Rrim_I_all | 0.114 |
Rpim _reflns.pdbx_Rpim_I_all | 0.034 |
| Total number of observations | - |
Total number unique _reflns.number_obs | 18680 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 20.50 |
Completeness [%] _reflns.percent_possible_obs | 99.7 |
Multiplicity _reflns.pdbx_redundancy | 21.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 7L17 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2020-12-14 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 29.9 - 3.050 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2594 / 0.2935 |
Structure solution method _refine.pdbx_method_to_determine_struct | SAD |