Data quality metrics extracted from 1k24.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1K24 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
ESRF BEAMLINE ID14-2
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
ESRF
Beamline
_diffrn_source.pdbx_synchrotron_beamline
ID14-2
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
1999-10-09
Detector
_diffrn_detector.type
MARRESEARCH
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.934
Software
Data reduction
_software.classification
MOSFLM
Data scaling
_software.classification
CCP4 (SCALA)
Phasing
_software.classification
SHARP
Refinement
_software.classification
REFMAC
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
96.859 46.346 73.977 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.93400 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 36.500 2.080
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.030 2.030
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.084 0.325
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 21875 1320
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 16.50 4.10
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 98.3 82.4
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 10.2 6.2
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1K24
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2001-09-26
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
36.5 - 2.030 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2350 / 0.2740
Structure solution method
_refine.pdbx_method_to_determine_struct
MIR