| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | MAD |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | NSLS BEAMLINE X12C |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | NSLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X12C |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2001-03-20 |
Detector _diffrn_detector.type | BRANDEIS - B1 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 1.28322, 1.28356, 1.23985 |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling _software.classification | SCALEPACK |
Phasing _software.classification | SHARP |
Refinement _software.classification | X-PLOR (3.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 36.528 85.096 88.036 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.283221.283561.23985 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1JOC |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2001-07-27 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 20.0 - 2.200 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2210 / 0.2810 |
Structure solution method _refine.pdbx_method_to_determine_struct | MAD |