| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | EMBL/DESY, HAMBURG |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X11 |
Temperature [K] _diffrn.ambient_temp | 260 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2004-01-27 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data reduction _software.classification | H |
Data scaling _software.classification | SCALEPACK |
Phasing _software.classification | REFMAC |
Refinement _software.classification | REFMAC (5.2.0005) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | I 2 2 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 103.144 130.758 159.992 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.81150 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 50.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.990 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.150 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 20662 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 93.5 |
Multiplicity _reflns.pdbx_redundancy | 5.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2JBK |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2006-12-07 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 100.0 - 2.990 Å |
R _refine.ls_R_factor_obs | 0.2100 |
Rwork _refine.ls_R_factor_R_work | 0.2100 WARNING: no Rfree given? |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | PDB ENTRY 2C6C |