Data quality metrics extracted from 1ipe.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1IPE at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
LAUE
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
ESRF BEAMLINE ID14-3
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
ESRF
Beamline
_diffrn_source.pdbx_synchrotron_beamline
ID14-3
Temperature [K]
_diffrn.ambient_temp
288.0
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
1998-12-11
Detector
_diffrn_detector.type
FUJI
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.7-1.65
Software
Data collection
_software.classification
INTLAUE
Data reduction #1
_software.classification
LAUENORM
Data reduction #2
_software.classification
INTLAUE
Data scaling
_software.classification
LAUENORM
Phasing
_software.classification
X-PLOR (3.851)
Model building
_software.classification
X-PLOR (3.851)
Refinement
_software.classification
X-PLOR (3.851)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 61 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
88.6 88.6 338.9 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.700001.65000 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 43.000 2.590
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.500 2.500
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.134 0.280
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 24496 -
  <I/σ(I)> - -
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 85.9 82.8
Multiplicity 
_reflns.pdbx_redundancy
 6.1 -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1IPE
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2001-05-09
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
10.0 - 2.500 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1950 / 0.2680