Data quality metrics extracted from 2iob.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2IOB at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SPRING-8 BEAMLINE BL12B2
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SPring-8
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL12B2
Temperature [K]
_diffrn.ambient_temp
200
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2004-11-11
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9797, 0.9799, 0.9537
Software
Data collection
_software.classification
HKL-2000
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
HKL-2000
Phasing
_software.classification
SOLVE
Refinement
_software.classification
XTALVIEW
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 1 2 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
149.267 92.964 108.296 90.000 109.373 90.000
Wavelength
_diffrn_radiation_wavelength.wavelength
1.000000.979700.979900.95370 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 50.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.200
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.076
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 70953
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 18.80
  Completeness [%] -
Multiplicity 
_reflns.pdbx_redundancy
 4.1
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
2IOB
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2006-10-10
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
50.0 - 2.200 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1755 / 0.2360
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD