Data quality metrics extracted from 2il9.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2IL9 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
ROTATING ANODE
Source details
_diffrn_source.type
RIGAKU
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
ALS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
8.2.1
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
2006-05-29
Detector
_diffrn_detector.type
RIGAKU RAXIS IV
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.5418
Software
Data collection
_software.classification
CrystalClear (MSC/RIGAKU)
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
HKL-2000
Phasing
_software.classification
SOLVE (2.03; 20-Sept-2002; Tom Terwilliger; terwilliger@LANL.gov)
Refinement
_software.classification
CNS (1.1; Axel T. Brunger; axel.brunger@yale.edu)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 63
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
133.570 133.570 160.425 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.105301.105701.100401.54180 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 16.970
High resolution limit [Å] 
_reflns.d_resolution_high
 3.100
  Rmerge -
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 26973
  <I/σ(I)> -
  Completeness [%] -
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
2IL9
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2006-10-02
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
17.0 - 3.100 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2530 / 0.2940
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD