| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | CHESS BEAMLINE F1 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | CHESS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | F1 |
Temperature [K] _diffrn.ambient_temp | 277.00 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1993-09-15 |
Detector _diffrn_detector.type | FUJI |
| Software | |
Data collection _software.classification | PURDUE (SOFTWARE) |
Data reduction _software.classification | PURDUE (SOFTWARE) |
Data scaling _software.classification | PURDUE (DATA PROCESSING PACKAGE) |
Phasing _software.classification | PURDUE (AVERAGING PROGRAM) |
Model building _software.classification | PURDUE (AVERAGING PROGRAM) |
Refinement _software.classification | NONE |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 267.6 268.5 274.3 61.9 62.6 60.2 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 15.000 |
High resolution limit [Å] _reflns.d_resolution_high | 3.500 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.090 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
| Total number unique | - |
| <I/σ(I)> | - |
| Completeness [%] | - |
Multiplicity _reflns.pdbx_redundancy | 1.2 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1IJS |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-09-12 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | CANINE PARVOVIRUS (MONOCLINIC P21) |