| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | LAUE |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | NSLS BEAMLINE X26C |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | NSLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X26C |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1993-10-15 |
Detector _diffrn_detector.type | FUJI |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.7 - 2.1 |
| Software | |
Data reduction _software.classification | OXFORD (LAUE PACKAGE (J.CAMPBELL)) |
Phasing _software.classification | X-PLOR (3.1) |
Model building _software.classification | X-PLOR (3.1) |
Refinement _software.classification | X-PLOR (3.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 43 21 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 105.1 105.1 150.3 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.700002.10000 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1IDE |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-01-18 |
R _refine.ls_R_factor_obs | 0.1920 |
Rwork _refine.ls_R_factor_R_work | 0.1920 WARNING: no Rfree given? |