| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | APS BEAMLINE 24-ID-E |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | APS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | 24-ID-E |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2006-01-10 |
Detector _diffrn_detector.type | ADSC QUANTUM 315 |
| Software | |
Refinement _software.classification | REFMAC (5.3.0036) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 76.2 114.7 123.0 84.1 81.2 80.7 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.03944 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 30.000 |
High resolution limit [Å] _reflns.d_resolution_high | 3.250 |
Rmerge _reflns.pdbx_Rsym_value | 0.042 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 60983 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 96.2 |
Multiplicity _reflns.pdbx_redundancy | 1.8 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 3I6W |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2009-07-07 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 30.0 - 3.250 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2510 / 0.2870 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | 3I6U |