Data quality metrics extracted from 6i5m.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 6I5M at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
ROTATING ANODE
Source details
_diffrn_source.type
BRUKER AXS MICROSTAR
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2013-04-03
Detector
_diffrn_detector.type
Bruker Platinum 135
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.54179
Software
Data reduction
_software.classification
PROTEUM PLUS
Data scaling
_software.classification
PROTEUM PLUS
Phasing
_software.classification
PHASER
Refinement
_software.classification
PHENIX (1.10.1_2155: ???)
General information
Spacegroup name
_symmetry.space_group_name_H-M
H 3 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
142.143 142.143 218.587 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.54179 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 27.243 2.500
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.400 2.400
Rmerge 
_reflns.pdbx_Rsym_value _reflns_shell.pdbx_Rsym_value
 0.084 0.336
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_obs
 33014 3784
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 10.28 2.16
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 98.7 99.2
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 2.9 2.8
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
6I5M
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2018-11-13
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
27.2 - 2.400 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1728 / 0.2242
Structure solution method
_refine.pdbx_method_to_determine_struct
MOLECULAR REPLACEMENT
Starting model (for MR)
_refine.pdbx_starting_model
4M4S