Data quality metrics extracted from 4hzn.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 4HZN at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 21-ID-D
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
21-ID-D
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2009-06-08
Detector
_diffrn_detector.type
MARMOSAIC 300 mm CCD
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97941, 1.127
Software
Data collection
_software.classification
HKL-2000
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
SOLVE
Refinement
_software.classification
REFMAC (5.5.0109)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 61 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
60.165 60.165 311.193 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979411.12700 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 28.060
High resolution limit [Å] 
_reflns.d_resolution_high
 2.250
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.074
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 16907
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 28.70
Completeness [%] 
_reflns.percent_possible_obs
 98.8
Multiplicity 
_reflns.pdbx_redundancy
 17.3
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
4HZN
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2012-11-15
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
28.1 - 2.250 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1998 / 0.2538
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD