| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | MAD |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | ESRF BEAMLINE ID14-2 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | ESRF |
Beamline _diffrn_source.pdbx_synchrotron_beamline | ID14-2 |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2000-01-01 |
Detector _diffrn_detector.type | ADSC QUANTUM 4 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.93260 |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling _software.classification | SCALEPACK |
Phasing #1 _software.classification | SOLVE |
Phasing #2 _software.classification | MLPHARE |
Model building #1 _software.classification | WARP |
Model building #2 _software.classification | ARP/wARP |
Refinement _software.classification | CNS (1.0) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 32 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 71.40 71.40 61.85 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.978580.978730.93260 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1HZT |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2001-01-26 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 23.4 - 1.450 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1920 / 0.2240 |
Structure solution method _refine.pdbx_method_to_determine_struct | AB INITIO PHASING |