| Experiment | |
|---|---|
Method _exptl.method | FIBER DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | APS BEAMLINE 18-ID |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | APS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | 18-ID |
Temperature [K] _diffrn.ambient_temp | 298.0 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1998-11-15 |
Detector _diffrn_detector.type | FUJI |
| Software | |
Refinement _software.classification | CNS |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 39.97 26.95 677.90 89.24 94.59 105.58 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.03000 Å |
| Data quality metrics | Overall | OuterShell |
|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 112.600 | 112.600 |
High resolution limit [Å] _reflns.d_resolution_high _reflns_shell.d_res_high | 5.160 | 5.160 |
| Rmerge | - | - |
| Rmeas | - | - |
| Rpim | - | - |
| Total number of observations | - | - |
Total number unique _reflns.number_obs | 424 | - |
| <I/σ(I)> | - | - |
Completeness [%] _reflns.percent_possible_obs _reflns_shell.percent_possible_all | 97.0 | 97.0 |
| Multiplicity | - | - |
| CC(1/2) | - | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 3HR2 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2009-06-08 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 112.6 - 5.160 Å |
R _refine.ls_R_factor_obs | 0.0420 |
Rwork _refine.ls_R_factor_R_work | 0.0420 WARNING: no Rfree given? |
Structure solution method _refine.pdbx_method_to_determine_struct | MIR |