| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | LURE BEAMLINE DW32 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | LURE |
Beamline _diffrn_source.pdbx_synchrotron_beamline | DW32 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1994-07 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data reduction _software.classification | MOSFLM (V. 5.21) |
Phasing _software.classification | X-PLOR |
Model building _software.classification | X-PLOR |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 43 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 88.87 88.87 97.96 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.90100 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1GRI |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-02-28 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 8.0 - 3.100 Å |
R _refine.ls_R_factor_obs | 0.2130 |
Rwork _refine.ls_R_factor_R_work | 0.2130 WARNING: no Rfree given? |