| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Temperature [K] _diffrn.ambient_temp | 300 |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1993-08-10 |
Detector _diffrn_detector.type | ENRAF-NONIUS FAST |
| Software | |
Data reduction _software.classification | MADNES |
Data scaling _software.classification | CCP4 |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 63.15 83.59 53.80 90.00 99.34 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 22.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.480 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.096 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 15818 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 76.5 |
Multiplicity _reflns.pdbx_redundancy | 2.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1GLI |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-02-22 |
Structure solution method _refine.pdbx_method_to_determine_struct | MUTANT-NATIVE DIFFERENCE MAP STARTING MODEL FOR MOLECULAR REPLACEMENT: NULL |
Starting model (for MR) _refine.pdbx_starting_model | WARNING: no starting model (for MR) given |