Data quality metrics extracted from 1gij.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1GIJ at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
PHOTON FACTORY BEAMLINE BL-6B
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
Photon Factory
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL-6B
Temperature [K]
_diffrn.ambient_temp
294
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
2000-07-07
Software
Data reduction
_software.classification
DENZO
Data scaling
_software.classification
CCP4
Phasing
_software.classification
AMoRE
Refinement
_software.classification
X-PLOR (98.0)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
74.020 72.069 53.982 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.00000 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 100.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.200
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.060
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 14195
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 17.60
Completeness [%] 
_reflns.percent_possible_obs
 92.3
Multiplicity 
_reflns.pdbx_redundancy
 4.1
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1GIJ
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2001-02-06
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
8.0 - 2.200 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2280 / 0.2860