| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Temperature [K] _diffrn.ambient_temp | 113.00 |
Collection date _diffrn_detector.pdbx_collection_date | 1994-04-01 |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling _software.classification | SCALEPACK |
Refinement _software.classification | X-PLOR (3.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 113.0 157.0 37.2 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 30.000 |
High resolution limit [Å] _reflns.d_resolution_high | 3.000 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.077 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 13255 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 94.2 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1GDT |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-04-11 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 3.000 Å |
R _refine.ls_R_factor_obs | 0.2350 |
Rwork _refine.ls_R_factor_R_work | 0.2350 WARNING: no Rfree given? |