| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1994-08-30 |
Detector _diffrn_detector.type | RIGAKU AFC-6R |
| Software | |
Data collection _software.classification | RIGAKU (AFC5 CONTROL SOFTWARE) |
Data reduction _software.classification | RIGAKU (AFC5 CONTROL SOFTWARE) |
Phasing _software.classification | X-PLOR (3.1) |
Model building _software.classification | X-PLOR (3.1) |
Refinement _software.classification | X-PLOR (3.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 32 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 66.37 66.37 80.28 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 17.500 |
High resolution limit [Å] _reflns.d_resolution_high | 2.200 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 11361 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 87.0 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1GBH |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-09-06 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 17.5 - 2.200 Å |
R _refine.ls_R_factor_obs | 0.1490 |
Rwork _refine.ls_R_factor_R_work | 0.1490 WARNING: no Rfree given? |