Data quality metrics extracted from 1g8j.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1G8J at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SSRL BEAMLINE BL9-2
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SSRL
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL9-2
Temperature [K]
_diffrn.ambient_temp
110
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
1999-04-30
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.797, 1.746, 1.742, 1.739, 0.98
Software
Data reduction #1
_software.classification
MOSFLM
Data reduction #2
_software.classification
TRUNCATE
Data scaling
_software.classification
CCP4 (TRUNCATE)
Phasing
_software.classification
SHARP
Refinement
_software.classification
CNS (1.0)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 1 21 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
96.71 114.25 108.98 90.00 112.44 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
1.797001.746001.742001.739000.98000 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 48.200
High resolution limit [Å] 
_reflns.d_resolution_high
 2.030
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.059
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 131366
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 16.40
Completeness [%] 
_reflns.percent_possible_obs
 93.2
Multiplicity 
_reflns.pdbx_redundancy
 4.0
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1G8J
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2000-11-17
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
20.0 - 2.030 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1930 / 0.2230
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD