| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | LAUE |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | ESRF BEAMLINE ID09 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | ESRF |
Beamline _diffrn_source.pdbx_synchrotron_beamline | ID09 |
Temperature [K] _diffrn.ambient_temp | 283.0 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2002-04-01 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data scaling #1 _software.classification | LAUEGEN |
Data scaling #2 _software.classification | PROW |
Data scaling #3 _software.classification | LSCALE |
Phasing _software.classification | CNS |
Refinement _software.classification | CNS (1.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 6 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 91.20 91.20 45.87 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.79000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 29.884 |
High resolution limit [Å] _reflns.d_resolution_high | 1.801 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 18357 |
| <I/σ(I)> | - |
| Completeness [%] | - |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2G0X |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2006-02-13 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 12.7 - 1.950 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.0550 / 0.0630 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | PDB ENTRY: 2SPL |