Data quality metrics extracted from 2g0b.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2G0B at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 8-BM
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
8-BM
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2003-07-16
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9795, 0.9422, 0.9793
Software
Data reduction
_software.classification
MOSFLM
Data scaling #1
_software.classification
SCALA (CCP4_3.1.20; 6/11/2002; Phil Evans; pre@mrc-lmb.cam.ac.uk)
Data scaling #2
_software.classification
CCP4 (SCALA)
Phasing #1
_software.classification
SHARP (de La Fortelle; sharp-develop@globalphasing.com)
Phasing #2
_software.classification
DM (4.2; 26/11/98; K. Cowtan; ccp4@dl.ac.uk)
Refinement
_software.classification
REFMAC (refmac_5.1.24; 24/04/2001; Murshudov, G.N.; ccp4@dl.ac.uk)
General information
Spacegroup name
_symmetry.space_group_name_H-M
I 41 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
182.832 182.832 287.429 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979500.942200.97930 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 129.100
High resolution limit [Å] 
_reflns.d_resolution_high
 3.000
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.081
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 48895
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 7.87
Completeness [%] 
_reflns.percent_possible_obs
 100.0
Multiplicity 
_reflns.pdbx_redundancy
 16.4
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
2G0B
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2006-02-11
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
29.8 - 3.000 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2550 / 0.2920
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD