Data quality metrics extracted from 2fzv.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2FZV at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 8-BM
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
8-BM
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2005-12-11
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97949
Software
Data collection
_software.classification
MAR345
Data scaling #1
_software.classification
XDS
Data scaling #2
_software.classification
SCALEPACK
Phasing
_software.classification
SHARP
Refinement
_software.classification
REFMAC (5.2.0005)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 43 21 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
117.821 117.821 154.080 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.946440.97949 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 29.810 1.800
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 1.700 1.700
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.029 0.240
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 116180 17520
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 38.33 5.68
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 97.6 94.7
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 5.8 3.6
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
2FZV
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2006-02-10
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
29.8 - 1.700 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1988 / 0.2458
Structure solution method
_refine.pdbx_method_to_determine_struct
SIRAS