| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SRS BEAMLINE PX9.6 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SRS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | PX9.6 |
Temperature [K] _diffrn.ambient_temp | 297 |
Collection date _diffrn_detector.pdbx_collection_date | 1996-02 |
| Software | |
Phasing _software.classification | PHASES |
Refinement _software.classification | X-PLOR (3.843) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 107.72 48.08 167.56 90.0 105.7 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.87000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 30.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.900 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.145 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 35552 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 87.1 |
Multiplicity _reflns.pdbx_redundancy | 8.9 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1FZA |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-08-05 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 30.0 - 2.900 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2630 / 0.3630 |
Structure solution method _refine.pdbx_method_to_determine_struct | ISOMORPHOUS REPLACEMENT |