| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | PHOTON FACTORY BEAMLINE BL-18B |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Photon Factory |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL-18B |
Temperature [K] _diffrn.ambient_temp | 298 |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1996-12-15 |
Detector _diffrn_detector.type | WEISSENBERG |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling _software.classification | SCALEPACK |
Phasing #1 _software.classification | MLPHARE |
Phasing #2 _software.classification | DM |
Model building _software.classification | DM |
Refinement _software.classification | REFMAC |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | I 2 2 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 117.6 248.4 82.7 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.00000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 100.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.800 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.069 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 28509 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 93.3 |
Multiplicity _reflns.pdbx_redundancy | 3.6 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1FIY |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-05-02 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.800 Å |
R _refine.ls_R_factor_obs | 0.2190 WARNING: no Rwork given |
Rfree _refine.ls_R_factor_R_free | 0.2590 |
Structure solution method _refine.pdbx_method_to_determine_struct | MULTIPLE ISOMORPHOUS REPLACEMENT |