Data quality metrics extracted from 2fbn.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2FBN at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
ROTATING ANODE
Source details
_diffrn_source.type
RIGAKU RU200
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
2005-12-07
Detector
_diffrn_detector.type
RIGAKU RAXIS IV
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
2.29
Software
Data reduction
_software.classification
CrystalClear (MSC/RIGAKU)
Data scaling
_software.classification
HKL-2000
Phasing #1
_software.classification
SOLVE
Phasing #2
_software.classification
RESOLVE
Model building #1
_software.classification
ARP/wARP
Model building #2
_software.classification
Coot (V. 0.0.33)
Refinement
_software.classification
REFMAC (5.2.0019)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
56.239 62.936 103.334 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.541802.29000 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 50.000 1.660
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 1.630 1.630
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.043 0.507
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 41003 720
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 19.40 1.64
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 88.0 31.0
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 6.0 2.9
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
2FBN
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-12-09
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
50.0 - 1.630 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1998 / 0.2352
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD