Data quality metrics extracted from 1f4c.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1F4C at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
ROTATING ANODE
Source details
_diffrn_source.type
RIGAKU RUH3R
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
1999-02-18
Detector
_diffrn_detector.type
RIGAKU RAXIS IV
Software
Data scaling
_software.classification
d*TREK
Phasing
_software.classification
AMoRE
Refinement
_software.classification
REFMAC
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 63
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
126.22 126.22 67.02 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.54180 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 10.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.000
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.044
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 41001
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 14.70
Completeness [%] 
_reflns.percent_possible_obs
 98.8
Multiplicity 
_reflns.pdbx_redundancy
 2.4
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1F4C
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2000-06-07
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
10.0 - 2.000 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1980 / 0.2680