Data quality metrics extracted from 2f2e.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2F2E at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 19-ID
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
19-ID
Collection date
_diffrn_detector.pdbx_collection_date
2005-04-01
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97932, 0.97948
Software
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
SOLVE
Refinement
_software.classification
REFMAC (5.2.0005)
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 1 2 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
46.884 78.865 78.941 90.00 91.64 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979320.97948 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 78.000
High resolution limit [Å] 
_reflns.d_resolution_high
 1.850
  Rmerge -
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 24599
  <I/σ(I)> -
  Completeness [%] -
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
2F2E
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-11-16
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
35.3 - 1.850 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1770 / 0.2510
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD