| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU |
Temperature [K] _diffrn.ambient_temp | 115 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1998-10-02 |
Detector _diffrn_detector.type | RIGAKU RAXIS IV |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling _software.classification | SCALEPACK |
Phasing _software.classification | RAVE |
Model building _software.classification | RAVE |
Refinement _software.classification | X-PLOR (3.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 42 3 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 336.0 336.0 336.0 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall | OuterShell |
|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 8.000 | 3.100 |
High resolution limit [Å] _reflns_shell.d_res_high | - | 3.000 |
| - | - | |
Rmerge _reflns_shell.Rmerge_I_obs | - | 0.131 |
| Rmeas | - | - |
| Rpim | - | - |
| Total number of observations | - | - |
| Total number unique | - | - |
| <I/σ(I)> | - | - |
Completeness [%] _reflns_shell.percent_possible_all | - | 18.6 |
| Multiplicity | - | - |
| CC(1/2) | - | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1F15 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2000-05-18 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 8.0 - 3.200 Å |
R _refine.ls_R_factor_obs | 0.2460 WARNING: neither Rwork nor Rfree given |