| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1993-09-20 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data collection _software.classification | MARRESEARCH |
Data reduction _software.classification | MAR |
Phasing _software.classification | SHELXL-93 |
Model building _software.classification | SHELXL-93 |
Refinement _software.classification | SHELXL-93 |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 53.91 23.10 23.10 90.0 110.4 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.71070 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 25.260 |
High resolution limit [Å] _reflns.d_resolution_high | 1.000 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.054 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 13659 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 93.8 |
Multiplicity _reflns.pdbx_redundancy | 7.5 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2ERL |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-12-20 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 25.2 - 1.000 Å |
R _refine.ls_R_factor_obs | 0.1290 WARNING: no Rwork given |
Rfree _refine.ls_R_factor_R_free | 0.1650 |