Data quality metrics extracted from 6eqt.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 6EQT at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SLS BEAMLINE X10SA
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SLS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
X10SA
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
PIXEL
Collection date
_diffrn_detector.pdbx_collection_date
2016-09-29
Detector
_diffrn_detector.type
DECTRIS PILATUS 6M
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97793
Software
Data reduction
_software.classification
XSCALE
Data scaling
_software.classification
XSCALE
Phasing
_software.classification
PHENIX
Refinement
_software.classification
REFMAC (5.8.0135)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 41
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
87.3 87.3 81.1 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.97793 Å

Data quality metricsOverallInnerShellOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 87.300 87.300 2.810
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.735 12.230 2.735
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.077 0.044 1.461
Rmeas 
_reflns.pdbx_Rrim_I_all _reflns_shell.pdbx_Rrim_I_all
 0.082 0.047 1.551
  Rpim - - -
Total number of observations 
_reflns.pdbx_number_measured_all _reflns_shell.number_measured_obs
 152272 1454 10344
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_obs
 16182 191 1172
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 17.28 46.41 1.37
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 99.8 97.9 98.5
Multiplicity 
_reflns.pdbx_redundancy
 9.4 - -
  CC(1/2) - - -

Refinement
PDB entry ID
_entry.id
6EQT
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2017-10-15
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
87.3 - 2.735 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2056 / 0.2538
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD