| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU RU200 |
Temperature [K] _diffrn.ambient_temp | 289 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1999-09-14 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data reduction _software.classification | MOSFLM |
Data scaling #1 _software.classification | SCALA |
Data scaling #2 _software.classification | CCP4 (SCALA) |
Phasing _software.classification | EPMR |
Refinement _software.classification | MAIN |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 2 2 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 62.251 92.480 209.876 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 13.400 |
High resolution limit [Å] _reflns.d_resolution_high | 2.670 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.062 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 16732 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 11.90 |
Completeness [%] _reflns.percent_possible_obs | 95.0 |
Multiplicity _reflns.pdbx_redundancy | 9.1 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1EF7 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2000-02-07 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.670 Å |
R _refine.ls_R_factor_obs | 0.1830 WARNING: no Rwork given |
Rfree _refine.ls_R_factor_R_free | 0.2260 |