| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU RU200 |
Temperature [K] _diffrn.ambient_temp | 300 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1996-09 |
Detector _diffrn_detector.type | RIGAKU |
| Software | |
Data reduction _software.classification | MOSFLM |
Refinement _software.classification | TNT (5E) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 64.87 31.00 35.29 90.00 105.63 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 15.340 |
High resolution limit [Å] _reflns.d_resolution_high | 1.700 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 14099 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 97.0 |
Multiplicity _reflns.pdbx_redundancy | 2.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1EBC |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1999-03-04 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 15.3 - 1.800 Å |
Structure solution method _refine.pdbx_method_to_determine_struct | OTHER |