| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | BRUKER AXS MICROSTAR |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2011-03-15 |
Detector _diffrn_detector.type | Bruker Platinum 135 |
| Software | |
Data collection _software.classification | PROTEUM PLUS |
Data reduction _software.classification | PROTEUM PLUS |
Data scaling _software.classification | PROTEUM PLUS |
Phasing _software.classification | MOLREP |
Refinement _software.classification | REFMAC (5.5.0109) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 35.873 36.302 47.474 85.84 77.21 68.24 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 46.290 |
High resolution limit [Å] _reflns.d_resolution_high | 2.750 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 5422 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 96.2 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 4E9D |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2012-03-21 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 46.3 - 2.750 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2669 / 0.3298 |
Structure solution method _refine.pdbx_method_to_determine_struct | 3P2Z |