Data quality metrics extracted from 1e4e.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1E4E at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
ROTATING ANODE
Temperature [K]
_diffrn.ambient_temp
120.0
Collection date
_diffrn_detector.pdbx_collection_date
1998-01-15
Software
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
MOLREP
Refinement
_software.classification
REFMAC
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 2 2 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
123.204 225.359 72.439 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.54180 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 15.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.500
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.058
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 32814
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 29.90
Completeness [%] 
_reflns.percent_possible_obs
 93.3
Multiplicity 
_reflns.pdbx_redundancy
 1.0
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1E4E
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2000-07-03
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
15.0 - 2.500 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1830 / 0.2570
Structure solution method
_refine.pdbx_method_to_determine_struct
MOLECULAR REPLACEMENT
Starting model (for MR)
_refine.pdbx_starting_model
PDB ENTRY 1IOW