| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Detector technology _diffrn_detector.detector | FILM |
Collection date _diffrn_detector.pdbx_collection_date | 1987-01-01 |
| Software | |
Data collection _software.classification | PURDUE (SOFTWARE) |
Data reduction _software.classification | PURDUE (DATA PROCESSING PACKAGE) |
Refinement _software.classification | TNT |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 263.21 349.01 267.32 90.00 90.82 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 999.900 |
High resolution limit [Å] _reflns.d_resolution_high | 2.900 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.122 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 565088 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 43.0 |
Multiplicity _reflns.pdbx_redundancy | 1.7 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 4DPV |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-02-01 |
Rfree _refine.ls_R_factor_R_free | 0.2830 WARNING: no Rwork given (but Rfree)!? |