| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Photon Factory |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL-6A |
Temperature [K] _diffrn.ambient_temp | 277 |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1992-10-23 |
Detector _diffrn_detector.type | WEISSENBERG |
| Software | |
Data reduction #1 _software.classification | BIOMOL |
Data reduction #2 _software.classification | WEIS |
Data scaling #1 _software.classification | WEIS |
Data scaling #2 _software.classification | BIOMOL |
Phasing #1 _software.classification | MLPHARE |
Phasing #2 _software.classification | BRUTE |
Phasing #3 _software.classification | DEMON |
Model building #1 _software.classification | BRUTE |
Model building #2 _software.classification | DEMON |
Refinement #1 _software.classification | TNT |
Refinement #2 _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 133.05 147.46 83.04 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.00000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 10.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.500 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 47612 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 83.1 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1DM0 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1999-12-13 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.500 Å |
R _refine.ls_R_factor_obs | 0.2060 |
Rwork _refine.ls_R_factor_R_work | 0.2060 WARNING: no Rfree given? |