Data quality metrics extracted from 5dlb.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 5DLB at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 24-ID-C
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
24-ID-C
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2014-08-13
Detector
_diffrn_detector.type
ADSC QUANTUM 315
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.0702
Software
Data reduction
_software.classification
XDS
Data scaling
_software.classification
XSCALE
Phasing
_software.classification
SHELX
Refinement
_software.classification
REFMAC (5.8.0049)
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 1 2 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
112.206 46.019 58.006 90.00 92.24 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
1.07020 Å

Data quality metricsOverallInnerShellOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 57.960 57.960 1.660
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 1.770 4.370 1.550
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.066 0.030 1.646
Rmeas 
_reflns.pdbx_Rrim_I_all _reflns_shell.pdbx_Rrim_I_all
 0.063 0.043 2.221
  Rpim - - -
Total number of observations 
_reflns.pdbx_number_measured_all _reflns_shell.number_measured_obs
 137146 5221 22985
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_obs
 25746 3043 12979
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 12.60 22.08 0.39
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 89.0 81.0 85.1
Multiplicity 
_reflns.pdbx_redundancy
 3.2 - -
  CC(1/2) - - -

Refinement
PDB entry ID
_entry.id
5DLB
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2015-09-04
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
58.0 - 1.770 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2089 / 0.2446
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD