| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SRS BEAMLINE PX9.6 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SRS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | PX9.6 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1995-11-16 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data reduction _software.classification | MOSFLM |
Phasing _software.classification | CCP4 |
Model building _software.classification | CCP4 |
Refinement _software.classification | TNT (5E) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | F 41 3 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 398.03 398.03 398.03 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.87000 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1DJI |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-09-25 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.500 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2200 / 0.2800 |
Structure solution method _refine.pdbx_method_to_determine_struct | DIFFERENCE FOURIER |