| Experiment | |
|---|---|
Method _exptl.method | ELECTRON CRYSTALLOGRAPHY |
Collection date _diffrn_detector.pdbx_collection_date | 2020-08-26 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.0197 |
| Software | |
Data scaling _software.classification | XSCALE (Wolfgang Kabsch) |
Refinement _software.classification | PHENIX (1.12_2829) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 69.98 174.02 199.45 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.01970 Å |
| Data quality metrics | Overall | InnerShell | OuterShell |
|---|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 131.126 | 131.126 | 3.180 |
High resolution limit [Å] _reflns.d_resolution_high _reflns_shell.d_res_high | 3.000 | 9.000 | 3.000 |
Rmerge _reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs | 1.159 | 0.557 | 1.786 |
Rmeas _reflns.pdbx_Rrim_I_all _reflns_shell.pdbx_Rrim_I_all | 1.173 | 0.566 | 1.808 |
| Rpim | - | - | - |
Total number of observations _reflns.pdbx_number_measured_all _reflns_shell.number_measured_obs | 1783075 | 67253 | 275487 |
Total number unique _reflns.number_obs _reflns_shell.number_unique_obs | 40941 | 1641 | 6529 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs | 3.79 | 7.54 | 1.90 |
Completeness [%] _reflns.percent_possible_obs _reflns_shell.percent_possible_all | 82.3 | 80.8 | 82.7 |
Multiplicity _reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy | 43.6 | 41.0 | 42.2 |
CC(1/2) _reflns.pdbx_CC_half _reflns_shell.pdbx_CC_half | 0.688 | 0.941 | 0.185 |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 7DI8 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2020-11-18 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 131.1 - 3.200 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.3089 / 0.3482 |