Data quality metrics extracted from 2deo.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2DEO at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
PHOTON FACTORY BEAMLINE BL-6A
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
Photon Factory
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL-6A
Temperature [K]
_diffrn.ambient_temp
100.0
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2004-12-19
Detector
_diffrn_detector.type
ADSC QUAMTUM 4r
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9789, 0.9792, 0.9900
Software
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
SHARP
Refinement
_software.classification
CNS (1.1)
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 1 2 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
103.212 108.400 59.342 90.00 110.06 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
0.978900.979200.99000 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 20.000
High resolution limit [Å] 
_reflns.d_resolution_high
 3.000
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.067
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 12407
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 25.20
Completeness [%] 
_reflns.percent_possible_obs
 100.0
Multiplicity 
_reflns.pdbx_redundancy
 3.8
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
2DEO
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2006-02-16
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
19.8 - 3.000 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1980 / 0.2420
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD