| Experiment | |
|---|---|
Method _exptl.method | ELECTRON CRYSTALLOGRAPHY |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ELECTRON MICROSCOPE |
Detector technology _diffrn_detector.detector | POSITION SENSITIVE DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 2021-12-14 |
Detector _diffrn_detector.type | TVIPS TEMCAM-F416 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.0197 |
| Software | |
Data reduction _software.classification | XDS (Wolfgang Kabsch; Wolfgang.Kabsch@mpimf-heidelberg.mpg.de) |
Data scaling _software.classification | XSCALE (Wolfgang Kabsch) |
Phasing _software.classification | SHELXD |
Refinement _software.classification | PHENIX (Paul D. Adams; PDAdams@lbl.gov) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 23.14 4.84 19.79 90.000 107.048 90.000 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.01970 Å |
| Data quality metrics | Overall | InnerShell | OuterShell |
|---|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 18.920 | 8.000 | 1.000 |
High resolution limit [Å] _reflns.d_resolution_high _reflns_shell.d_res_high | 0.900 | 5.000 | 0.900 |
Rmerge _reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs | 0.113 | 0.034 | 0.322 |
Rmeas _reflns.pdbx_Rrim_I_all _reflns_shell.pdbx_Rrim_I_all | 0.129 | 0.047 | 0.366 |
| Rpim | - | - | - |
Total number of observations _reflns.pdbx_number_measured_all _reflns_shell.number_measured_obs | 5980 | 8 | 1639 |
Total number unique _reflns.number_obs _reflns_shell.number_unique_obs | 1237 | 3 | 332 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs | 8.63 | 13.06 | 5.01 |
Completeness [%] _reflns.percent_possible_obs _reflns_shell.percent_possible_all | 71.0 | 50.0 | 72.2 |
Multiplicity _reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy | 4.8 | 2.7 | 4.9 |
CC(1/2) _reflns.pdbx_CC_half _reflns_shell.pdbx_CC_half | 0.991 | 1.000 | 0.643 |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 8DDG |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2022-06-18 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 5.8 - 0.900 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1692 / 0.1851 |
Structure solution method _refine.pdbx_method_to_determine_struct | FOURIER SYNTHESIS |