Data quality metrics extracted from 1d8a.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1D8A at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SRS BEAMLINE PX7.2
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SRS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
PX7.2
Temperature [K]
_diffrn.ambient_temp
298
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
1998-09-25
Detector
_diffrn_detector.type
MARRESEARCH
Software
Data reduction
_software.classification
DENZO
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
TNT
Refinement
_software.classification
TNT
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 61 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
80.6 80.6 327.6 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.48800 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 999.000 2.240
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.200 2.180
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.057 -
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 153843 -
  <I/σ(I)> - -
Completeness [%] 
_reflns.percent_possible_obs
 78.0 -
  Multiplicity - -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1D8A
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
1999-10-21
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
20.0 - 2.200 Å
Rfree
_refine.ls_R_factor_R_free
0.2940
WARNING: no Rwork given (but Rfree)!?