Data quality metrics extracted from 2d3q.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2D3Q at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
PHOTON FACTORY BEAMLINE BL-6A
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
Photon Factory
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL-6A
Temperature [K]
_diffrn.ambient_temp
95
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2005-02-25
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.0
Software
Data collection
_software.classification
CrystalClear
Data reduction #1
_software.classification
TRUNCATE
Data reduction #2
_software.classification
CrystalClear (MSC/RIGAKU)
Data scaling
_software.classification
CCP4 (TRUNCATE)
Phasing
_software.classification
MLPHARE
Refinement
_software.classification
CNS (1.1)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 65 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
136.212 136.212 363.596 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.700001.00000 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 25.000 2.330
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.250 2.250
  Rmerge - -
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 89434 -
  <I/σ(I)> - -
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 94.1 68.4
  Multiplicity - -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
2D3Q
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-09-30
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
25.0 - 2.800 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2340 / 0.2670
Structure solution method
_refine.pdbx_method_to_determine_struct
MIR